Journal article
Bestimmung von deoxynivalenol mittels LC - MS/MS (Tandem Massenspektrometrie)
Mycotoxin research, v 18 Suppl 1(S1), pp 52-55
Mar 2002
PMID: 23606094
Abstract
A sensitive and selective method using high-performance liquid chromatography in combination with atmospheric pressure chemical ionization tandem mass spetrometry (LC-APCI-MS/MS) has been developed for the determination of Deoxynivalenol (DON) in trace levels. The extract was purified with a MultiSep™ column followed by the Vicam™ DON immunoaffinity column. Quantification is based on an external standard method using positive Multiple Reaction Monitoring (MRM). The limit of detection was 5 μg/kg with a signal to noise ratio of 3:1.
Metrics
3 Record Views
1 citations in Scopus
Details
- Title
- Bestimmung von deoxynivalenol mittels LC - MS/MS (Tandem Massenspektrometrie)
- Creators
- O Kappenstein - Bundesinstitut für gesundheitlichen Verbraucherschutz und Veterinärmedizin, Thielallee 88-92, 14195, BerlinH St KlaffkeHj SpottR TiebachR Weber
- Publication Details
- Mycotoxin research, v 18 Suppl 1(S1), pp 52-55
- Publisher
- Springer Nature; Germany
- Resource Type
- Journal article
- Language
- German
- Scopus ID
- 2-s2.0-84859623750
- Other Identifier
- 991014877698504721