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Confirmation of Dynamically Recrystallized Grains in Hexagonal Zirconium through Local Internal Friction Measurements
Journal article

Confirmation of Dynamically Recrystallized Grains in Hexagonal Zirconium through Local Internal Friction Measurements

K. S. Thool, K. V. Mani Krishna, D. Srivastava, A. Patra, R. D. Doherty and I. Samajdar
Metallurgical and materials transactions. A, Physical metallurgy and materials science, v 50A(11), pp 5000-5014
01 Nov 2019

Abstract

Materials Science Materials Science, Multidisciplinary Metallurgy & Metallurgical Engineering Science & Technology Technology
Fully recrystallized hexagonal Zirconium was subjected to controlled hot compression tests. Deformation above 723 K showed both flow saturation, characteristic of dynamic recovery, and also the presence of fine equiaxed grains, indicating dynamic recrystallization (DRx). Though data from relative work hardening were inconclusive, a combination of transmission Kikuchi diffraction plus transmission electron microscopy clearly confirmed the presence of DRx grains. A separation between the deformed and the DRx grains was not possible with microtexture or nano-indentation data. Local internal friction measurements (or tan delta values), however, clearly distinguished the DRx grains from both statically recrystallized (SRex) and the hot deformed grains. (C) The Minerals, Metals & Materials Society and ASM International 2019

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Web of Science research areas
Materials Science, Multidisciplinary
Metallurgy & Metallurgical Engineering
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