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Edge Capping of 2D‐MXene Sheets with Polyanionic Salts To Mitigate Oxidation in Aqueous Colloidal Suspensions
Journal article   Peer reviewed

Edge Capping of 2D‐MXene Sheets with Polyanionic Salts To Mitigate Oxidation in Aqueous Colloidal Suspensions

Varun Natu, James L. Hart, Maxim Sokol, Helen Chiang, Mitra L. Taheri and Michel W. Barsoum
Angewandte Chemie (International ed.), v 58(36), pp 12655-12660
02 Sep 2019
PMID: 31293049

Abstract

2D materials functionalization MXenes oxidation ESI Highly Cited Paper (Incites)
MXenes have shown promise in myriad applications, such as energy storage, catalysis, EMI shielding, among many others. However, MXene oxidation in aqueous colloidal suspensions when stored in water at ambient conditions remains a challenge. It is now shown that by simply capping the edges of individual MXene flakes, Ti3C2Tz and V2CTz, by polyanions such as polyphosphates, polysilicates or polyborates, it is possible to quite significantly reduce their propensity for oxidation even when held in aerated water for weeks. This breakthrough resulted from the realization that the edges of MXene sheets are positively charged. It is thus an example of selectively functionalizing the edges differently from the MXene sheet surfaces. Stability by capping: MXenes generally tend to oxidize when stored as a colloid in water at ambient conditions. Capping the edges of individual MXene flakes by polyanions, however, significantly decreases the rate of oxidation, and makes long‐term storage of MXene possible. This is important because it renders solution processing of MXenes scalable and facile.

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Web of Science research areas
Chemistry, Multidisciplinary
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