Logo image
Effect of cation off-stoichiometry on optical absorption in epitaxial LaFeO 3 films
Journal article   Peer reviewed

Effect of cation off-stoichiometry on optical absorption in epitaxial LaFeO 3 films

Mark D. Scafetta and Steven J. May
Physical chemistry chemical physics : PCCP, v 19(16), pp 10371-10376
2017
PMID: 28379257

Abstract

We have investigated the effect of La and Fe deficiency on the c -axis lattice parameter and optical absorption in La 1−x Fe 1−y O 3−δ films deposited by oxide MBE. La deficient films display minimal changes in optical and structural properties compared with stoichiometric LaFeO 3 , even with relatively large cation vacancy concentrations (∼22%). Fe deficient films show a linear increase in c -axis parameter with increasing Fe vacancy concentration. The optical absorption coefficient is reduced for Fe deficient films over the spectral range from 1.2 to 5.0 eV. This leads to a relatively simple and effective method to quantify the approximate Fe deficiency in LaFeO 3 . Minimal changes in optical and structural properties are observed when cation deficient films are exposed to strongly oxidizing (ozone annealing) conditions. This indicates a strong accompaniment of charge balancing oxygen vacancies to maintain a nominal Fe 3+ valence state, acting to stabilize the band structure even in the presence of significant cation off-stoichiometry.

Metrics

12 Record Views
22 citations in Scopus

Details

InCites Highlights

Data related to this publication, from InCites Benchmarking & Analytics tool:

Web of Science research areas
Chemistry, Physical
Physics, Atomic, Molecular & Chemical
Logo image