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Fabrication of porous carbon nanofibers with adjustable pore sizes as electrodes for supercapacitors
Journal article   Peer reviewed

Fabrication of porous carbon nanofibers with adjustable pore sizes as electrodes for supercapacitors

Chau Tran and Vibha Kalra
Journal of power sources, v 235, pp 289-296
01 Aug 2013

Abstract

Chemistry Chemistry, Physical Electrochemistry Energy & Fuels Materials Science Materials Science, Multidisciplinary Physical Sciences Science & Technology Technology
We report a facile method for obtaining extremely high surface area and uniformly porous carbon nanofibers for supercapacitors. Blends of polyacrylonitrile and sacrificial Nafion at different compositions have been electrospun into non-woven nanofiber mats with diameters in the range of 200-400 nm. Electrospun nanofiber mats are then subjected to carbonization to obtain porous carbon nanofibers (CNFs) as polyacrylonitrile converts to carbon and Nafion decomposes out creating intra-fiber pores. Resultant porous CNFs exhibit specific surface area of up to 1600 m(2) g(-1) with a large fraction of mesopores (2-4 nm). No additional chemical or physical activation process was used. We demonstrate the tunability of the pore sizes within CNFs by varying the amount of Nafion. The non-woven fiber mats of porous CNFs are studied as free-standing electrode materials for supercapacitors eliminating the need for polymeric binding agents. Electrochemical measurements showed large specific gravimetric and volumetric capacitances of up to 210 F g(-1) and 60 F cm(-3) in 1 M H2SO4 at a high cyclic voltammetry scan rate of 100 mV s(-1) due to the large fraction of mesopores. These materials retain 75% performance at a large current density of 20 A g(-1) indicating excellent power handling capability. (C) 2013 Elsevier B.V. All rights reserved.

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Web of Science research areas
Chemistry, Physical
Electrochemistry
Energy & Fuels
Materials Science, Multidisciplinary
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