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Fast airborne sulfur dioxide measurements by Atmospheric Pressure Ionization Mass Spectrometry (APIMS)
Journal article   Open access   Peer reviewed

Fast airborne sulfur dioxide measurements by Atmospheric Pressure Ionization Mass Spectrometry (APIMS)

Donald C. Thornton, Alan R. Bandy, Fang H. Tu, Byron W. Blomquist, Glenn M. Mitchell, Wolfgang Nadler and Donald H. Lenschow
Journal of Geophysical Research: Atmospheres, v 107(D22), pp ACH 13-1-ACH 13-10
27 Nov 2002
url
https://doi.org/10.1029/2002jd002289View
Published, Version of Record (VoR)Maybe Open Access (Publisher Bronze) Open
url
https://doi.org/10.1029/2002JD002289View
Published, Version of Record (VoR) Open

Abstract

eddy correlation mass spectrometry sulfur dioxide
An atmospheric pressure ionization mass spectrometer (APIMS) was developed to determine atmospheric sulfur dioxide (SO2). High precision and immunity to sample loss, fluctuations in instrument sensitivity, etc., were achieved by adding isotopically labeled SO2 (34S16O2) continuously to the manifold as an internal standard. During the NASA Transport And Chemical Evolution Over The Pacific (TRACE P) program and the National Science Foundation (NSF) Passing Efficiency of the Low Turbulence Inlet (PELTI) program, 32S16O2 and 34S16O2 were each determined with integration times of 20 ms. From these data the ambient SO2 level was computed every 40 ms. In the PELTI studies at SO2 levels of approximately 60 parts per trillion by volume (pptv), vertical fluxes were determined with a precision better than 10%. When the data were averaged to 1 s, the lower limit of detection was <1 pptv at the 2σ level. Isotopomer ratios observed during the Aerosol Characterization Experiment—Asia (ACE Asia), intercomparisons of APIMS and gas chromatography/mass spectrometry with isotopically labeled internal standard on the same aircraft in test flights and PELTI, and the intercomparison of two APIMS instruments on different aircraft during ACE Asia and TRACE P, are presented to support the high sensitivity, accuracy, specificity, and high time response of the instrument.

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Meteorology & Atmospheric Sciences
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