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Highly Photoluminescent and Stable Aqueous ZnS Quantum Dots
Journal article   Open access   Peer reviewed

Highly Photoluminescent and Stable Aqueous ZnS Quantum Dots

Hui Li, Wan Y Shih and Wei-Heng Shih
Industrial & engineering chemistry research, v 49(2), pp 579-582
2010
PMID: 21954321
url
https://doi.org/10.1021/ie901086dView
Published, Version of Record (VoR) Open

Abstract

We report an all-aqueous synthesis of highly photoluminescent and stable ZnS quantum dots (QDs) with water as the medium, i.e. first synthesizing ZnS QDs with 3-mercaptopropionic acid (MPA) as the capping molecule, followed by replacing some of MPA with (3-mercaptopropyl) trimethoxysilane (MPS). The resultant MPS-replaced ZnS QDs were about 5 nm in size with a cubic zinc blende crystalline structure, and had both MPA and MPS on the surface as confirmed by the Fourier Transform Infrared (FTIR) spectroscopy. They exhibited blue trap-state emissions around 415 nm and a quantum yield (QY) of 75% with Rhodamine 101 as the reference, and remained stable for more than 60 days under the ambient conditions. Through the capping molecule replacement procedure, the MPS-replaced ZnS QDs avoided the shortcomings of both the MPA-ZnS QDs and the MPS-ZnS QDs, and acquired the advantages of strong photoluminescence and good stability, which are important to the QDs’ applications especially for bioimaging.

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Engineering, Chemical
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