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Increase of nanodiamond crystal size by selective oxidation
Journal article   Peer reviewed

Increase of nanodiamond crystal size by selective oxidation

S Osswald, M Havel, V Mochalin, G Yushin and Y Gogotsi
Diamond and related materials, v 17(7), pp 1122-1126
2008

Abstract

X-ray diffraction High resolution electron microscopy Oxidation Nanocrystalline diamond Raman spectroscopy
The control of the crystal size in nanodiamond (ND) powder is crucial, since most of its physical and chemical properties are size-related. In this work we demonstrate a simple method for increasing the crystal size of ND powder by selective oxidation in air. We analyze the oxidized powders by high-resolution transmission electron microscopy, X-ray diffraction and Raman spectroscopy in order to monitor changes in the average crystal size distribution and identify the limitations of these techniques for crystal size measurements. Our studies show that none of these techniques alone is able to provide sufficiently accurate information on size distributions, but can produce complementary results for better understanding of the properties of ND powder.

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Collaboration types
Domestic collaboration
Web of Science research areas
Materials Science, Coatings & Films
Materials Science, Multidisciplinary
Physics, Applied
Physics, Condensed Matter
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