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Nanoporous metals from thermal decomposition of transition metal dichalcogenides
Journal article   Peer reviewed

Nanoporous metals from thermal decomposition of transition metal dichalcogenides

Swarnendu Chatterjee, Anton Anikin, Debjit Ghoshal, James L. Hart, Yawei Li, Saad Intikhab, D. A. Chareev, O. S. Volkova, A. N. Vasiliev, Mitra L. Taheri, …
Acta materialia, v 184
01 Feb 2020

Abstract

Materials Science Materials Science, Multidisciplinary Metallurgy & Metallurgical Engineering Science & Technology Technology
Nanoporous metals (np-M) have emerged as promising materials owing to their high surface area-tovolume ratio and electrical thermal conductivity. There exists a group of processing methodologies by which np-M are formed through a top-down nanostructure evolution driven by the selective removal of a sacrificial component, all of which are a variation of dealloying. Nanoporosity evolution through current dealloying methodologies, however, is governed by strict requirements including sufficient separation in "reactivity" of the participating components and a homogeneous solid solution precursor alloy. This limits the viable alloy systems that may be used and the range of np-M's that may be formed. Here, we report thermal decomposition of crystalline transition metal dichalcogenides (TMDs) as a new processing methodology for np-M formation, adding to the spectrum of dealloying protocols. We demonstrate application of this process to the formation of a broader class of np-M including W, Re, Mo, and Ta with feature sizes below 100 nm. The presented facile thermal treatment of TMDs offers a new methodology for the evolution of nanoporosity in a broad range of metals. (C) 2019 Acta Materialia Inc. Published by Elsevier Ltd. All rights reserved.

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Web of Science research areas
Materials Science, Multidisciplinary
Metallurgy & Metallurgical Engineering
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