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Quantitative Correlation between Bound Water and Mechanical Stress Relaxation in Dehydrated Metal-Coordinate Polymer Networks
Journal article   Peer reviewed

Quantitative Correlation between Bound Water and Mechanical Stress Relaxation in Dehydrated Metal-Coordinate Polymer Networks

Sungjin Kim, Myungwoon Lee, Mei Hong and Niels Holten-Andersen
Chemistry of materials, v 34(23), pp 10329-10337
13 Dec 2022

Abstract

Chemistry Chemistry, Physical Materials Science Materials Science, Multidisciplinary Physical Sciences Science & Technology Technology
Dynamic metal-coordinate cross-links impart smart and superior physicochemical properties in their deployments in many biological and artificial metallopolymer networks in various stages of solidification via dehydration. Nonetheless, a quantitative model that describes to what extent the dynamic behaviors of metal-coordinate bond transition from the hydrated to the dehydrated state is missing. In previous work, we have shown that local water binding helps metal-coordinate bonds to maintain their dynamic properties during bulk network dehydration, thereby offering mechanical damping properties to the network deep into the dehydrated solid state. Using mussel-inspired hydrogels with chemically tuned fractions of metal-coordinate cross-links, here, we reveal the direct scaling relationship between the macroscopic relaxation time of the dehydrated network and the amount of microscopic water bound by metal-coordinate cross-links. This quantitative relationship between dehydrated metal-coordinate network mechanics and metal-coordinate cross-link dynamics may help us better understand and emulate the sustainable process of solidification via spatiotemporally controlled dehydration of load-bearing materials on wide display in nature.

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Collaboration types
Domestic collaboration
Web of Science research areas
Chemistry, Physical
Materials Science, Multidisciplinary
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